OBT751 Syllabus - Analytical Methods And Instrumentation - 2017 Regulation - Open Elective | Anna University
OBT751 Syllabus - Analytical Methods And Instrumentation - 2017 Regulation - Open Elective | Anna University
OBT751 |
ANALYTICAL METHODS AND INSTRUMENTATION |
L T P C |
---|
3003
UNIT I |
SPECTROMETRY |
9 |
---|
Properties of electromagnetic radiation- wave properties – components of optical instruments– Sources of radiation – wavelength selectors – sample containers – radiation transducers – Signal process and read outs – signal to noise ratio - sources of noise – Enhancement of signal to noise - types of optical instruments – Applications
UNIT II |
MOLECULAR SPECTROSCOPY |
9 |
---|
Molecular absorption spectrometry – Measurement of Transmittance and Absorbance – Beer’s law – Instrumentation - Applications -Theory of fluorescence and Phosphorescence –Theory of Infrared absorption spectrometry – IR instrumentation – Applications – Theory of Raman spectroscopy – Instrumentation – applications
UNIT III |
NMR AND MASS SPECTROMETRY |
9 |
---|
Theory of NMR –– chemical shift- NMR-spectrometers – applications of 1H and 13C NMR- Molecular mass spectra – ion sources. Mass spectrometer. Applications of molecular mass - Electron paramagnetic resonance- g values – instrumentation
UNIT IV |
SEPARATION METHODS |
9 |
---|
General description of chromatography – Band broadening and optimization of column performance- Liquid chromatography – Partition chromatography – Adsorption chromatography – Ion exchange chromatography -size exclusion chromatography- Affinity chromatography- principles of GC and applications – HPLC- Capillary electrophoresis – Applications
UNIT V |
ELECTRO ANALYSIS AND SURFACE MICROSCOPY |
9 |
---|
Electrochemical cells- Electrode potential cell potentials – potentiometry- reference electrode – ion selective and molecular selective electrodes – Instrument for potentiometric studies – Voltametry – Cyclic and pulse voltametry- Applications of voltametry . Study of surfaces – Scanning probe microscopes – AFM and STM.
TOTAL: 45 PERIODS
TEXT BOOKS:
1. Skoog, D.A. F. James Holler, and Stanky, R.Crouch “Instrumental Methods of Analysis”.Cengage Learning , 2007.
2. Willard, Hobart, etal., “Instrumental Methods of Analysis”. VIIth Edition, CBS, 1986.
3. Braun, Robert D. “ Introduction to Instrumental Analysis”. Pharma Book Syndicate, 1987.
4. Ewing,G.W. “Instrumental Methods of Chemical Analysis”, Vth Edition, McGraw-Hill, 1985
2. Willard, Hobart, etal., “Instrumental Methods of Analysis”. VIIth Edition, CBS, 1986.
3. Braun, Robert D. “ Introduction to Instrumental Analysis”. Pharma Book Syndicate, 1987.
4. Ewing,G.W. “Instrumental Methods of Chemical Analysis”, Vth Edition, McGraw-Hill, 1985
REFERENCES:
1. Sharma, B.K. “Instrumental Methods of Chemical Analysis : Analytical Chemistry” GoelPublishing House, 1972.
2. Haven, Mary C., etal., “Laboratory Instrumentation “. IVth Edition, John Wiley, 1995.
2. Haven, Mary C., etal., “Laboratory Instrumentation “. IVth Edition, John Wiley, 1995.
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